KoffyKraft · Thumpassery Estate

The Citane Process Compass

A stage-by-stage field guide to coffee leaf processing — from harvest to final moisture reduction. Each stage documents the key parameters, decision points, pitfalls, and the reasoning behind each choice.

Contents

  1. 1 · Harvest
  2. 2 · Transfer and Holding
  3. 3 · Surface Preparation
  4. 4 · Wither
  5. 5 · Manipulation
  6. 6 · Reaction Window
  7. 7 · Moisture Reduction
  8. 8 · QC Checkpoints
Published Research — peer-reviewed, cited
Traditional Practice — documented, not formally validated
Citane Adaptation — unpublished, estate observation
1

Harvest

Timing · Maturity · Handling

Leaf maturity at harvest is the single most consequential decision in the entire process. It determines which volatile compounds are available, which enzymes are active, and which processing pathways are possible downstream.

Maturity Reference
MaturityKey CompoundsSuitable Pathways
Young flush (1–3 months)Highest mangiferin · hexanal · (E,Z)-2,6-nonadienal · Low tanninGreen · Refreshing · Floral · Oolong
Mid-maturity (3–5 months)Balanced chlorogenic acids · Moderate β-ionone precursorsWidest range — Oolong · White · Yeast ferment · Floral
Mature (5–7 months)High tannin · High lipid · Low green volatilesBlack · Roast · Smoke · Decoction
Post-mature / yellowDegraded chlorophyll · Elevated β-carotene breakdown productsHoney-ionone pathway only · Not suitable for green
Harvest Protocol
Harvest in early morning — leaf temperature is lower, enzyme activity slower, reduced risk of field oxidation before processing begins.
Do not harvest wet leaves (after rain or heavy dew) for green or oolong style — surface moisture accelerates unwanted fermentation before enzyme arrest can be achieved.

2

Transfer and Holding

Container · Atmosphere · Time window

The transfer window — time between harvest and first processing step — is an active period. Enzymes begin working the moment the leaf is cut. Managing this window determines whether you arrive at the next stage with the chemistry you intended.

Time Window Decisions
If your target isThen
Green / Refreshing profileProcess within 30 min of harvest. No holding. Steaming must begin immediately.
Oolong / Floral / SweetAllow 0–2h ambient hold. This is the beginning of the wither window.
Black / Woody / DecoctionHold up to 4h acceptable. Mature leaves are more tolerant.
Unavoidable delay (>2h for green target)Refrigerate at 4–8°C. Cold holds enzyme activity. Resume within 6h.
Container Requirements
Sealed containers + warm ambient temperature (Kerala 28–32°C) = uncontrolled fermentation within 1–2h. If fermentation is not the intended process, this is a critical quality loss point.

3

Surface Preparation

Wash decision · Contamination · Compound integrity

Whether to wash — and how — is a genuine decision with compound-level consequences. Water contact initiates cell surface reactions. The correct protocol depends on what comes next.

Wash Decision
SituationProtocol
Light field dust only, green targetLight brush or dry wipe only. No water.
Moderate contamination, green targetBrief mist rinse (spray bottle). Pat dry immediately. Do not soak.
Oolong / black / ferment targetQuick rinse acceptable. Remove excess moisture before wither.
Decoction target (Engere / Chemo style)Rinse acceptable — compounds extracted in brew water; surface moisture not critical.
Heavily contaminated leavesRedirect to secondary batch for decoction profile. Do not use for green or oolong.
Never soak leaves destined for green or refreshing profiles. Soaking causes rapid intracellular damage through osmotic pressure. Green volatile compounds (hexanal, (E,Z)-2,6-nonadienal) are destroyed before processing begins. ● Steger et al. 2022 confirmed soaking as a quality loss pathway.

4

Wither

Time · Temperature · Atmosphere · Profile commitment

Withering is the first intentional transformation stage. It controls the extent of enzymatic oxidation before any heat treatment. Duration and temperature together determine which volatile families develop. This is where process style is committed.

Wither Parameters by Target Profile
StyleDuration / TempWhat happens
Green (JGTP / CGTP)0h — immediate enzyme arrestNo withering at all. Preserves hexanal, (E,Z)-2,6-nonadienal intact.
White / Sun-dried (WTP)12–24h, ambient, sun or shadeSlow enzymatic conversion. β-ionone and α-ionone precursors develop. Floral, sweet potential.
Oolong (OTP)12–24h, 22–25°C, shade or indoorPartial oxidation window. OCLT-exclusive compounds develop (limonene, diphenyl sulfone). Optimal: 24h. ● Fibrianto et al. 2025
Black (BTP)24h, ambientFull oxidation commitment. Tannin polymerisation proceeds. Woody, earthy character emerges.
Yeast fermentation path12–18h before inoculationPrimes leaf substrate. Partial enzyme activation before anaerobic switch.
Shade wither ○ Citane12–24h, low light, 22–25°CSlower than sun wither. More controlled ionone development without UV-driven carotenoid degradation.
Wither Atmosphere
Withering above 30°C accelerates oxidation past the intended window — oolong-target leaves can enter black-style oxidation within 6–8h instead of 24h. Monitor ambient temperature, especially in Kerala monsoon season when night temperatures remain high.

5

Manipulation

Rolling · Wring · Cell rupture · Post-wring hold

Mechanical manipulation controls cell wall rupture — the release of intracellular compounds into contact with oxygen and each other. Too little and the substrate is not primed; too much and the oxidative cascade runs ahead of the intended profile.

Manipulation Type by Target
ManipulationTarget ProfileWhat it does
No manipulationWhite / Sun-dried / DecoctionWhole leaf drying. Minimal intracellular disruption. Flavour through surface chemistry only.
Blend / cutGreen / RefreshingHexanal and 4-heptenal released. Immediately followed by enzyme arrest (steam or oven).
Light roll (~10–15% rupture)Oolong / Floral / FruityReleases ionone precursors without full oxidative cascade. Moisture gradient created.
Medium wring (~30–40% rupture)Black / WoodySignificant tannin-enzyme contact. Full oxidation proceeding. Commit to black profile.
Wring Hold and Post-Wring Temperature

Wringing generates a small but measurable temperature increase in the leaf mass from mechanical energy. This post-wring temperature rise accelerates enzyme activity — intentionally or not.

Wring/roll intensity descriptions are observational field estimates, not validated measurements. % cell rupture requires microscopy to quantify. Label all wring-related protocols as Citane Adaptation (unpublished) until formally documented.

6

Reaction Window

Let run · Stall · Stop · Fermentation cascades

After manipulation, the leaf is in an active reactive state. The question is not whether reactions are happening — they always are — but whether to let them run, stall them at a chosen point, or stop them entirely.

Reaction Control Decisions
IntentAction
Stop — Green targetSteam at 100°C, 2–3 min. Full enzyme arrest. Locks green volatile profile.
Stall — Oolong targetMonitor colour (green → yellow-green edge). Dry at 70°C when target reached.
Let run — Black targetAllow full 24h wither without interruption. Oven dry when leaves are copper-red.
Yeast fermentation ●Apply Saccharomyces cerevisiae starter (40mL per batch). Anaerobic, 25°C, 12h. Then dry. ● Steger et al. 2022
Wild fermentation ●No starter. Anaerobic hold, 25°C, 12h. Variable outcomes — document each batch. ● Steger et al. 2022
Koji fermentation ○Aspergillus oryzae inoculation. Humidity-controlled environment. Enzymatic pathway distinct from yeast. Theoretical — not yet formally documented for CLT.
Koji mist ○Light spray of Koji spore suspension on leaf surface. Partial surface inoculation. Theoretical.
Water soak activation ○Brief controlled soak (15–30 min, ambient) to activate surface enzymes then immediate arrest. Theoretical — requires testing.
Enzyme Temperature Reference
EnzymeActive / InactivatedRelevance
Polyphenol oxidase (PPO)Active 15–35°C · Inactivated >70°CPrimary oxidation enzyme. Controls green → black conversion.
PeroxidaseActive 20–40°C · Inactivated >80°CSecondary oxidation. More heat-resistant than PPO.
LipoxygenaseActive 15–30°C · Inactivated >60°CProduces green aldehydes (hexanal, etc). Steaming is effective arrest.
Protease / amylaseActive 20–50°CAmino acid and sugar release. Active during fermentation window.

7

Moisture Reduction

Method · Temperature · Duration · Target moisture

Moisture reduction arrests remaining enzyme activity through heat or desiccation, and stabilises the leaf for storage and brewing. The method affects volatile retention — high heat drives off aromatic compounds faster than low heat.

Drying Methods
MethodParametersNotes
Oven dry70°C / 4hStandard for green, oolong, black. ● Fibrianto et al. 2025 and Steger et al. 2022. Reliable enzyme arrest without excessive volatile loss.
Sun dry≥48h ambientWhite style and traditional pathways. Slow moisture loss preserves floral ionones. Weather-dependent — humidity risk.
Flat-pan roast (Kuti)High heat, 15–20 minSimultaneous drying and roast character development. Mature leaves only. Pyrazines and guaiacol formed. ◐ Klingel et al. 2020
Smoke-dry (Kawa Daun)2–4h, closed furnace, cassia woodSimultaneous drying and smoke infusion. Cinnamomum burmannii volatile oils absorbed into leaf. ◐ Novita et al. 2018
Air dry (low humidity)24–48h at 25°C with airflowGentler than oven. Suitable for wild fermentation outcomes where high heat may destroy fermentation-derived esters.
Target Moisture

8

QC Checkpoints

Brix · pH · Sensory · Documentation

Optional measurement points that help track process consistency across batches. None are mandatory at small scale — sensory assessment is the primary tool. Introduce instruments only where they add information that sensory cannot provide.

Measurement Reference
CheckpointWhenWhat it tells you
Brix (refractometer)After wither, before dryingTracks sugar concentration increase from moisture loss. Useful for wither consistency across batches. ○ Target Brix change: +2–4° over 24h wither (Citane estimate — not formally documented for CLT).
pH (meter or strips)After fermentation · After brewFermentation lowers pH as organic acids develop. Brew pH affects mouthfeel. CLT brew pH documented at 5.57–7.06 depending on altitude and variety. ● Fibrianto et al. 2024
Sensory — colourAfter wither · After dryingMost reliable visual process marker. Green → yellow-green (oolong window) → copper-red (black) → dark brown (roast).
Sensory — aromaAfter wither · After drying · After brewPrimary quality signal. Green aldehydes for green target. Floral-sweet for oolong. Off-notes: sour, musty, acrid = process failure.
Batch documentationAll stagesHarvest date/time, leaf maturity, wither start/end time and temp, manipulation type, fermentation duration, drying method and duration, final sensory notes. Repeat success requires documentation.
The single most important QC tool is a batch log. Without it, a successful batch cannot be reliably repeated and a failed batch cannot be diagnosed. A simple handwritten card per batch is sufficient.